Methanol → HCID 22601390, 화합물
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[C:1]1([NH:7][S:8]([C:11]2[CH:12]=[C:13]([CH:17]=[CH:18][CH:19]=2)[C:14](O)=[O:15])(=[O:10])=[O:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.B.C1COCC1.CO>C1COCC1>[OH:15][CH2:14][C:13]1[CH:12]=[C:11]([S:8]([NH:7][C:1]2[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=2)(=[O:10])=[O:9])[CH:19]=[CH:18][CH:17]=1참가 물질
5
실험 절차
To solution of 3-Phenylsulfamoyl-benzoic acid (380 mg, 1.36 mmol) in THF (10 ml) was added BH3.THF (1M, 5.4 ml, 5.4 mmol) dropwise. After the addition, the reaction mixture was allowed to stir for 3 d at room temperature. Methanol was added to the reaction and the mixture concentrated in vacuo (5×). This compound was used in the next step without further purification.
후처리
- additionAfter the addition
- concentrationthe mixture concentrated in vacuo (5×)
- customThis compound was used in the next step without further purification
출처 및 근거
- ORD 기록
- ord-1f5ecdacdbd748d0b7aba8d286d7ac2a
- 출처 데이터셋
- uspto-grants-2004_12
- 특허 번호
- US06835731B2
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