HCID 22601390, 화합물 → HCID 22601475, 화합물
반응식
[OH:1][CH2:2][C:3]1[CH:4]=[C:5]([S:9]([NH:12][C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)(=[O:11])=[O:10])[CH:6]=[CH:7][CH:8]=1>C(Cl)Cl.O=[Mn]=O>[CH:2]([C:3]1[CH:4]=[C:5]([S:9]([NH:12][C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)(=[O:11])=[O:10])[CH:6]=[CH:7][CH:8]=1)=[O:1]참가 물질
4
실험 절차
Reaction of 3-Hydroxymethyl-N-phenyl-benzenesulfonamide (crude from previous step, 1.36 mmol), MnO2 (1.40 g, 13.60 mmol) in CH2Cl2 (10 mL) at 40° C. under N2 overnight gave the title compound (293 mg, 82%) as a white solid.
출처 및 근거
- ORD 기록
- ord-8c86eed5e80144d3aab00561883a19c8
- 출처 데이터셋
- uspto-grants-2004_12
- 특허 번호
- US06835731B2
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