Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → 1-[2-(Benzyloxy)-6-hydroxyphenyl]ethan-1-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Benzyl Bromide | HCID 7498 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | 2',6'-Dihydroxyacetophenone | HCID 69687 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | 1-[2-(Benzyloxy)-6-hydroxyphenyl]ethan-1-one | HCID 2775187 | — |
반응 단계
To a mixture of 2′,6′-dihydroxyacetophenone (4 g) and potassium carbonate (3.82 g) in acetone (40 mL) was added benzyl bromide (3.13 mL), and the mixture was stirred at room temperature overnight. The reaction mixture was poured into water, and the precipitated crystals were collected by filtration. The crystals were washed with water and n-hexane, and dried under reduced pressure to give the title compound (3.67 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07566699B2 |
| 출처 데이터셋 | uspto-grants-2009_07 |
| ORD ID | ord-ad510b46ab0447c5abe0f9bfcbc6058e |
| 출처 메모 | uspto-grants-2009_07 |