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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 230869생성일: 2026년 10월 26일

Water → 1-[2-(Benzyloxy)-6-hydroxyphenyl]ethan-1-one

https://huagongshe.com/reaction/230869

반응식

참여 물질

역할이름HCID투입량
반응물WaterHCID 962—
반응물Benzyl BromideHCID 7498—
반응물Potassium CarbonateHCID 11430—
반응물2',6'-DihydroxyacetophenoneHCID 69687—
용매AcetoneHCID 180—
생성물1-[2-(Benzyloxy)-6-hydroxyphenyl]ethan-1-oneHCID 2775187—

반응 단계

To a mixture of 2′,6′-dihydroxyacetophenone (4 g) and potassium carbonate (3.82 g) in acetone (40 mL) was added benzyl bromide (3.13 mL), and the mixture was stirred at room temperature overnight. The reaction mixture was poured into water, and the precipitated crystals were collected by filtration. The crystals were washed with water and n-hexane, and dried under reduced pressure to give the title compound (3.67 g).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US07566699B2
출처 데이터셋uspto-grants-2009_07
ORD IDord-ad510b46ab0447c5abe0f9bfcbc6058e
출처 메모uspto-grants-2009_07