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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 230893생성일: 2026년 10월 25일

Water → 6'-Hydroxy-2'-(methoxycarbonylmethoxy)acetophenone

https://huagongshe.com/reaction/230893

반응식

참여 물질

역할이름HCID투입량
반응물WaterHCID 962—
반응물Potassium CarbonateHCID 11430—
반응물Methyl bromoacetateHCID 60984—
반응물2',6'-DihydroxyacetophenoneHCID 69687—
용매AcetoneHCID 180—
생성물6'-Hydroxy-2'-(methoxycarbonylmethoxy)acetophenoneHCID 10537084—

반응 단계

To a mixture of 2′,6′-dihydroxyacetophenone (6 g) and potassium carbonate (5.72 g) in acetone (20 mL) was added methyl bromoacetate (3.73 mL), and the mixture was stirred at room temperature for 5 days. To the reaction mixture was added water, and the precipitated crystals were collected by filtration. The crystals were washed with water and dried under reduced pressure to give the title compound (7.89 g).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US07566699B2
출처 데이터셋uspto-grants-2009_07
ORD IDord-9697439f8c5f4eaf8fdafdd370708a5d
출처 메모uspto-grants-2009_07