Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → 6'-Hydroxy-2'-(methoxycarbonylmethoxy)acetophenone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | Methyl bromoacetate | HCID 60984 | — |
| 반응물 | 2',6'-Dihydroxyacetophenone | HCID 69687 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | 6'-Hydroxy-2'-(methoxycarbonylmethoxy)acetophenone | HCID 10537084 | — |
반응 단계
To a mixture of 2′,6′-dihydroxyacetophenone (6 g) and potassium carbonate (5.72 g) in acetone (20 mL) was added methyl bromoacetate (3.73 mL), and the mixture was stirred at room temperature for 5 days. To the reaction mixture was added water, and the precipitated crystals were collected by filtration. The crystals were washed with water and dried under reduced pressure to give the title compound (7.89 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07566699B2 |
| 출처 데이터셋 | uspto-grants-2009_07 |
| ORD ID | ord-9697439f8c5f4eaf8fdafdd370708a5d |
| 출처 메모 | uspto-grants-2009_07 |