Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Chloro-2,4-Dinitrobenzene → 1-(2,4-Dinitrophenyl)-4,4'-bipyridinium chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Chloro-2,4-Dinitrobenzene | HCID 6 | — |
| 반응물 | 4,4'-Bipyridine | HCID 11107 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 1-(2,4-Dinitrophenyl)-4,4'-bipyridinium chloride | HCID 23021316 | 136.3% |
반응 단계
4,4′-Bipyridine (10 g, 0.065 moles) and chloro-2,4-dinitrobenzene (13 g, 0.065 moles) in ethanol (150 ml) in a 250 ml flask were refluxed for fifteen hours and allowed to cool. The ethanol was removed under vacuum and acetone (200 ml) was added and the mixture was stirred. The suspension was filtered and dried under vacuum to yield 1-(2,4-dinitrophenyl)-4,4′-bipyridinium chloride (17.5 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07567371B2 |
| 출처 데이터셋 | uspto-grants-2009_07 |
| ORD ID | ord-c01f28da0a0d4246adb696056705fbd5 |
| 출처 메모 | uspto-grants-2009_07 |