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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 230976생성일: 2026년 10월 23일

1-Chloro-2,4-Dinitrobenzene → 1-(2,4-Dinitrophenyl)-4,4'-bipyridinium chloride

https://huagongshe.com/ko/reaction/230976

반응식

참여 물질

역할이름HCID투입량
반응물1-Chloro-2,4-DinitrobenzeneHCID 6—
반응물4,4'-BipyridineHCID 11107—
용매EthanolHCID 702—
생성물1-(2,4-Dinitrophenyl)-4,4'-bipyridinium chlorideHCID 23021316136.3%

반응 단계

4,4′-Bipyridine (10 g, 0.065 moles) and chloro-2,4-dinitrobenzene (13 g, 0.065 moles) in ethanol (150 ml) in a 250 ml flask were refluxed for fifteen hours and allowed to cool. The ethanol was removed under vacuum and acetone (200 ml) was added and the mixture was stirred. The suspension was filtered and dried under vacuum to yield 1-(2,4-dinitrophenyl)-4,4′-bipyridinium chloride (17.5 g).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US07567371B2
출처 데이터셋uspto-grants-2009_07
ORD IDord-c01f28da0a0d4246adb696056705fbd5
출처 메모uspto-grants-2009_07