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Sodium Acetate → HCID 53937978, 화합물

HRID 230988
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HRID 230988 반응식
[C:1]([CH:6]1[C:11](=[O:12])[CH2:10][CH:9]([C:13]2[CH:18]=[CH:17][C:16]([CH2:19][CH2:20][CH3:21])=[CH:15][CH:14]=2)[CH2:8][C:7]1=[O:22])(=O)[CH2:2][CH2:3][CH3:4].[Cl-].[CH2:24]([O:26][NH3+:27])[CH3:25].C([O-])(=O)C.[Na+]>C(O)C>[CH2:24]([O:26][NH:27][CH2:4][CH2:3][CH2:2][CH:1]=[C:6]1[C:7](=[O:22])[CH2:8][CH:9]([C:13]2[CH:14]=[CH:15][C:16]([CH2:19][CH2:20][CH3:21])=[CH:17][CH:18]=2)[CH2:10][C:11]1=[O:12])[CH3:25]
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참가 물질

5

반응물 3

HCID 517045Sodium AcetateHCID 19001768HCID 19001768, 화합물HCID 20034301HCID 20034301, 화합물

생성물 1

HCID 53937978HCID 53937978, 화합물

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

15.0 parts by weight of 2-butyryl-5-(4-n-propylphenyl)-cyclohexane-1,3-dione is reacted with 5.1 parts by weight of ethoxyammonium chloride and 4.5 parts by weight of anhydroud sodium acetate in 120 parts by volume of ethanol, and worked up as in Example 1. There is obtained 2-(ethoxyaminobutylidene)-5-(4-n-propylphenyl)-cyclohexane-1,3-dione (active ingredient No. 4).

출처 및 근거

ORD 기록
ord-358edaca31a04663ad2729d3df526781
출처 데이터셋
uspto-grants-1989_07
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US04844735

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