Methyl 3-(3-hydroxypropyl)benzoate → Methyl 3-(3-oxopropyl)benzoate
반응식
[CH3:1][O:2][C:3]([C:5]1[CH:6]=[C:7]([CH2:11][CH2:12][CH2:13][OH:14])[CH:8]=[CH:9][CH:10]=1)=[O:4]>N1C=CC=CC=1.[O-2].[O-2].[O-2].[Cr+6]>[CH3:1][O:2][C:3]([C:5]1[CH:6]=[C:7]([CH2:11][CH2:12][CH:13]=[O:14])[CH:8]=[CH:9][CH:10]=1)=[O:4]참가 물질
4
실험 절차
3-(3-Methoxycarbonylphenyl)propanol (1.9 g) was oxidised with chromium trioxide (5.0 g) in pyridine (7.9 ml) as described in Example 1(e) to give the product as a pale oil.
출처 및 근거
- ORD 기록
- ord-49afc5a58e9a490f8ca2744f1c30ba39
- 출처 데이터셋
- uspto-grants-1989_07
- 특허 번호
- US04845110
반응 노트
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