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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 231284생성일: 2026년 10월 26일

Sodium hydroxide ethanol → Sodium butyl glycidyl phosphate

https://huagongshe.com/reaction/231284

반응식

참여 물질

역할이름HCID투입량
반응물Sodium hydroxide ethanolHCID 23692425—
반응물HCID 86743212HCID 86743212—
용매EthanolHCID 702—
생성물Sodium butyl glycidyl phosphateHCID 23698436100%

반응 조건

온도70 °C

반응 단계

50 g (0.19 mol) of sodium butyl 2-hydroxy-3chloropropyl phosphate was charged into a reactor, to which 1000 ml of ethanol was added, followed by agitation and heating to 70° C. to obtain a uniform mixture. Thereafter, the reaction system was cooled down to room temperature, to which was gradually added 88.6 g (0.19 mol) of a 0.0021 mol/g sodium hydroxide ethanol solution, followed by agitation for 3 hours while keeping the temperature. The HPLC analysis revealed the disappearance of a peak of the starting material with a peak for the resultant new product appearing. The resultant NaCl precipitate was removed by filtration and the ethanol was distilled off under reduced pressure to obtain 43 g (yield: 100%) of sodium butyl glycidyl phosphate.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US04845239
출처 데이터셋uspto-grants-1989_07
ORD IDord-e17e630651bc4823b01a22b74fce5162
출처 메모uspto-grants-1989_07