참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Sodium hydroxide ethanol | HCID 23692425 | — |
| 반응물 | HCID 86743212 | HCID 86743212 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | Sodium butyl glycidyl phosphate | HCID 23698436 | 100% |
반응 단계
50 g (0.19 mol) of sodium butyl 2-hydroxy-3chloropropyl phosphate was charged into a reactor, to which 1000 ml of ethanol was added, followed by agitation and heating to 70° C. to obtain a uniform mixture. Thereafter, the reaction system was cooled down to room temperature, to which was gradually added 88.6 g (0.19 mol) of a 0.0021 mol/g sodium hydroxide ethanol solution, followed by agitation for 3 hours while keeping the temperature. The HPLC analysis revealed the disappearance of a peak of the starting material with a peak for the resultant new product appearing. The resultant NaCl precipitate was removed by filtration and the ethanol was distilled off under reduced pressure to obtain 43 g (yield: 100%) of sodium butyl glycidyl phosphate.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US04845239 |
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| 출처 데이터셋 | uspto-grants-1989_07 |
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| ORD ID | ord-e17e630651bc4823b01a22b74fce5162 |
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| 출처 메모 | uspto-grants-1989_07 |
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