Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Aniline → 4-Phenyl-3,4-dihydroquinolin-2(1h)-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Aniline | HCID 6115 | — |
| 반응물 | 3-Phenylprop-2-enoyl chloride | HCID 66023 | — |
| 생성물 | 4-Phenyl-3,4-dihydroquinolin-2(1h)-one | HCID 272509 | — |
반응 단계
4-Phenyl-3,4-dihydrocarbostyril (CAS# 4888-33-9) was prepared in two steps using the procedure described by Conley, R. T.; Knopka. W. N. J. Org. Chem. 1964, 29, 496-497. The starting materials for this preparation were cinnamoyl chloride (Aldrich) and aniline (Aldrich). The title compound was purified by flash chromatography eluting with CH2Cl2/EtOAc (4:1).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06849650B2 |
| 출처 데이터셋 | uspto-grants-2005_02 |
| ORD ID | ord-eb44577bef4346a1b15aac443b94e8bc |
| 출처 메모 | uspto-grants-2005_02 |