Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzoyl Peroxide → (2,4-Dichloro-5-nitrophenyl)methyl bromide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzoyl Peroxide | HCID 7187 | — |
| 반응물 | N-bromobutanimide | HCID 67184 | — |
| 반응물 | 1,5-Dichloro-2-methyl-4-nitrobenzene | HCID 251679 | — |
| 용매 | Carbon Tetrachloride | HCID 5943 | — |
| 생성물 | (2,4-Dichloro-5-nitrophenyl)methyl bromide | HCID 14501785 | — |
반응 단계
This compound was prepared in a manner similar to Example 1 Step F using 2,4-dichloro-5-nitrotoluene (62.0 g, 0.3 mole), N-bromosuccinimide (160.2 g, 0.9 mole), benzoyl peroxide (2.0 g) and carbon tetrachloride (500 ml) to yield (2,4-dichloro-5-nitrophenyl)methyl bromide. The NMR spectrum was consistent with the proposed structure.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04846875 |
| 출처 데이터셋 | uspto-grants-1989_07 |
| ORD ID | ord-b2fd7d6809ae443fa2e3d2bbc9fa27eb |
| 출처 메모 | uspto-grants-1989_07 |