Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Amino-2-methyl-1-propanol → 2-[[(1-Oxo-1,3-dihydroisobenzofuran-5-yl)carbonyl]amino]-2-methyl-1-propanol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Amino-2-methyl-1-propanol | HCID 11807 | — |
| 반응물 | Ethyl 1,3-dihydro-1-oxoisobenzofuran-5-carboxylate | HCID 90088 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | 2-[[(1-Oxo-1,3-dihydroisobenzofuran-5-yl)carbonyl]amino]-2-methyl-1-propanol | HCID 11196005 | — |
반응 단계
Method B): 5-Ethoxycarbonylphthalid (82 g, 0.4 mole) is added to a solution of 2-amino-2-methylpropan-1-ol (44.6 g. 0.5 mole) in toluene (100 ml). The mixture is heated to reflux temperature for 24 hours. Upon cooling the title compound is filtered off and recrystallised from hot toluene.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06849749B2 |
| 출처 데이터셋 | uspto-grants-2005_02 |
| ORD ID | ord-b1c7e6f305a2432c90684e7fd8d07359 |
| 출처 메모 | uspto-grants-2005_02 |