3-Fluoro-3,3-dinitropropanol → 3-Fluoro-3,3-dinitropropyl pentafluorothioacetate

HRID 231917

반응식

HRID 231917 반응식
[F:1][C:2]([N+:9]([O-:11])=[O:10])([N+:6]([O-:8])=[O:7])[CH2:3][CH2:4][OH:5].[F:12][S:13]([F:20])=[C:14](O)[C:15]([F:18])([F:17])[F:16]>>[F:12][S:13]([F:20])=[C:14]([O:5][CH2:4][CH2:3][C:2]([F:1])([N+:9]([O-:11])=[O:10])[N+:6]([O-:8])=[O:7])[C:15]([F:18])([F:17])[F:16]

참가 물질

3

반응물 2

HCID 136153883-Fluoro-3,3-dinitropropanolHCID 86743239Pentafluorothioacetic acid

생성물 1

HCID 571702543-Fluoro-3,3-dinitropropyl pentafluorothioacetate수율 83%

실험 절차

Using a method similar to example 12, 3-fluoro-3,3-dinitropropanol and pentafluorothioacetic acid were reacted to form 3-fluoro-3,3-dinitropropyl pentafluorothioacetate (83% yield) mp 28° C.;

후처리

  1. customwere reacted

출처 및 근거

ORD 기록
ord-fcb24d67b2a34c63b4844e1a4c2e1cac
출처 데이터셋
uspto-grants-1989_07
특허 번호
US04849540

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