Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
P-Cresol → N-[2-(4-Methylphenoxy)ethyl]acetamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | P-Cresol | HCID 2879 | — |
| 반응물 | 2-Methyl-2-oxazoline | HCID 70713 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | N-[2-(4-Methylphenoxy)ethyl]acetamide | HCID 538338 | — |
반응 단계
Combine 5.0 g (0.046 mol) 4-methylphenol and 3.9 g (0.46 mol) 2-methyl-2-oxazoline under a nitrogen atmosphere and heat to 175° C. for 18 hours. After this time, cool the reaction mixture and add 50 mL of methylene chloride. Wash the organics with 3×10 mL of 10% potassium hydroxide, dry over sodium sulfate and remove the solvents to obtain the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04851526 |
| 출처 데이터셋 | uspto-grants-1989_07 |
| ORD ID | ord-7c51a4b7facc43c296c5d45e86fa81e8 |
| 출처 메모 | uspto-grants-1989_07 |