Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Chloride → 2,3,4,5-Tetrafluoro-6-methylbenzoyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Chloride | HCID 312 | — |
| 반응물 | 2,3,4,5-Tetrafluoro-6-methylbenzoic acid | HCID 12943997 | — |
| 생성물 | 2,3,4,5-Tetrafluoro-6-methylbenzoyl chloride | HCID 14651256 | — |
반응 단계
To 6-methyl-2,3,4,5-tetrafluorobenzoic acid (5.60 g) is added thiony chloride (9.8 ml) and the mixture is refluxed for 1 hour. After concentrating, 6-methyl-2,3,4,5-tetrafluorobenzoyl chloride (5.20 g) is obtained as a colorless oil, b.p. 82° C./23 mmHg.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05591744 |
| 출처 데이터셋 | uspto-grants-1997_01 |
| ORD ID | ord-e82a0650db9347bb99fe2fc522b08403 |
| 출처 메모 | uspto-grants-1997_01 |