참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 4-tert-Butylbenzylamine | HCID 2735655 | — |
| 반응물 | Ethyl 4-chloro-3-ethyl-1-methylpyrazole-5-carboxamide | HCID 54498586 | — |
| 생성물 | Tebufenpyrad | HCID 86354 | — |
반응 단계
A mixture of ethyl 4-chloro-3-ethyl-1-methylpyrazole-5-carboxamide and 4-tert-butylbenzylamine is heated to 200° C. for four hours with continuous stirring. Thereafter the reaction mixture is cooled to room temperature and the reaction mixture purified by silica gel chromatography to obtain the desired product 115°-117° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05591765 |
|---|
| 출처 데이터셋 | uspto-grants-1997_01 |
|---|
| ORD ID | ord-c599d53ad0804b5bbf9e2500d2967792 |
|---|
| 출처 메모 | uspto-grants-1997_01 |
|---|
