Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Cyclopentyloxy-4-methoxybenzaldehyde → 3-Cyclopentyloxy-4-methoxybenzyl alcohol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Cyclopentyloxy-4-methoxybenzaldehyde | HCID 2735893 | — |
| 반응물 | Sodium borohydride | HCID 4311764 | — |
| 용매 | Ethanol | HCID 702 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 3-Cyclopentyloxy-4-methoxybenzyl alcohol | HCID 11138706 | 98% |
반응 단계
A solution of 3-cyclopentyloxy-4-methoxybenzaldehyde (38 grams, 0.17 mol) in 40 milliliters of ethanol and sodium borohydride (1.63 grams,0.043 mol) was stirred for 2 hours at room temperature until complete by TLC. The reaction was diluted with water and extracted with ethyl acetate. Evaporation of the ethyl acetate afforded 3-cyclopentyloxy-4-methoxybenzyl alcohol (37 grams, 98%) suitable for the next step.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05591776 |
| 출처 데이터셋 | uspto-grants-1997_01 |
| ORD ID | ord-e738693e27a54e449d2f0766f81a7cbd |
| 출처 메모 | uspto-grants-1997_01 |