Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 232877생성일: 2026년 10월 26일
Ethanethiol → 2-(7-Chloro-6-ethylthioquinolin-2-yl)methoxy-11-oxo-6,11-dihydrodibenz[b,e]oxepine
https://huagongshe.com/reaction/232877
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Ethanethiol | HCID 6343 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | 2-(7-Chloro-6-fluoroquinolin-2-yl)methoxy-11-oxo-6,11-dihydrodibenz[b,e]oxepine | HCID 23359142 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | 2-(7-Chloro-6-ethylthioquinolin-2-yl)methoxy-11-oxo-6,11-dihydrodibenz[b,e]oxepine | HCID 23359231 | — |
반응 단계
0.37 ml of ethyl mercaptan and 1.12 g of potassium carbonate were added to 2.0 g of 2-(7-chloro-6-fluoroquinolin-2-yl)methoxy-11-oxo-6,11-dihydrodibenz[b,e]oxepine dissolved in 80 ml of dimethylformamide and the mixture was stirred at 90° C. for 4 hours.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05591752 |
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| 출처 데이터셋 | uspto-grants-1997_01 |
|---|
| ORD ID | ord-173c904036b3494ca7a6e3278b1b792f |
|---|
| 출처 메모 | uspto-grants-1997_01 |
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