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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 23311생성일: 2026년 10월 23일

Benzimidazole → Lithium benzimidazolate

https://huagongshe.com/ko/reaction/23311

반응식

참여 물질

역할이름HCID투입량
반응물BenzimidazoleHCID 5798—
반응물ButyllithiumHCID 178418339—
용매TolueneHCID 1140—
생성물Lithium benzimidazolateHCID 12985676—

반응 단계

A slurry of benzimidazole (8.50 g, 36.3 mmol) in toluene (40 mL) at 0° C. was treated with 25.8 mL of a 2.8 M n-BuLi (72.2 mmol) solution in hexanes. This solution mixture was then refluxed for one day during which time the slurry became off-white. The slurry was then filtered over a medium glass frit and dried to give a white solid.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US06852446B2
출처 데이터셋uspto-grants-2005_02
ORD IDord-a3fec071d6a44a0a9e0f5f1bd556fe97
출처 메모uspto-grants-2005_02