Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzimidazole → Lithium benzimidazolate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzimidazole | HCID 5798 | — |
| 반응물 | Butyllithium | HCID 178418339 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | Lithium benzimidazolate | HCID 12985676 | — |
반응 단계
A slurry of benzimidazole (8.50 g, 36.3 mmol) in toluene (40 mL) at 0° C. was treated with 25.8 mL of a 2.8 M n-BuLi (72.2 mmol) solution in hexanes. This solution mixture was then refluxed for one day during which time the slurry became off-white. The slurry was then filtered over a medium glass frit and dried to give a white solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06852446B2 |
| 출처 데이터셋 | uspto-grants-2005_02 |
| ORD ID | ord-a3fec071d6a44a0a9e0f5f1bd556fe97 |
| 출처 메모 | uspto-grants-2005_02 |