Trimethyl phosphite → Dimethyl [(3-methylphenyl)methyl]phosphonate

HRID 233442노트

반응식

HRID 233442 반응식
F[C:2]1[CH:14]=[CH:13][C:5]([CH2:6][P:7](=[O:12])([O:10][CH3:11])[O:8][CH3:9])=[CH:4][CH:3]=1.[CH3:15]C1C=C(C=CC=1)CBr.COP(OC)OC>>[CH3:15][C:3]1[CH:4]=[C:5]([CH:13]=[CH:14][CH:2]=1)[CH2:6][P:7](=[O:12])([O:10][CH3:11])[O:8][CH3:9]

참가 물질

4

반응물 3

HCID 8472Trimethyl phosphiteHCID 12099m-Xylyl bromideHCID 23208053HCID 23208053, 화합물

생성물 1

HCID 2773781Dimethyl [(3-methylphenyl)methyl]phosphonate

실험 절차

Following the procedure of Compound 11, 3-methylbenzyl bromide is reacted with trimethylphosphite.

출처 및 근거

ORD 기록
ord-d483430e27d04ed1bafcaeba34d043fc
출처 데이터셋
uspto-grants-1997_01
특허 번호
US05593980

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