Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Iodoethane → 2-Ethylbenzo[b]thiophene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Iodoethane | HCID 6340 | — |
| 반응물 | Benzo(B)Thiophene | HCID 7221 | — |
| 반응물 | HCID 178418306 | HCID 178418306 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | 2-Ethylbenzo[b]thiophene | HCID 595664 | — |
반응 단계
2-Ethylbenzo[b]thiophene was prepared by the method of Example 40A with benzo[b]thiophene (7.5 mmoles, 1.0 g), t-BuLi (1.7M, 8.9 mmoles, 5.3 ml), iodoethane (8.9 mmoles, 0.72 ml) and THF (20 ml). 1.2 g (99%) of a yellow liquid was isolated.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05594021 |
| 출처 데이터셋 | uspto-grants-1997_01 |
| ORD ID | ord-12ece86c36f14ae9b86f3487d2895506 |
| 출처 메모 | uspto-grants-1997_01 |