(3-Methoxyphenyl)boronic acid → HCID 22998523, 화합물

HRID 234372

반응식

HRID 234372 반응식
[CH3:1][O:2][C:3]1[CH:4]=[C:5](B(O)O)[CH:6]=[CH:7][CH:8]=1.Br[C:13]1[S:17][C:16]([S:18]([N:21]2[CH:25]=[CH:24][CH:23]=[CH:22]2)(=[O:20])=[O:19])=[CH:15][CH:14]=1>>[CH3:1][O:2][C:3]1[CH:4]=[C:5]([C:13]2[S:17][C:16]([S:18]([N:21]3[CH:25]=[CH:24][CH:23]=[CH:22]3)(=[O:19])=[O:20])=[CH:15][CH:14]=2)[CH:6]=[CH:7][CH:8]=1

참가 물질

3

반응물 2

HCID 2734370(3-Methoxyphenyl)boronic acidHCID 23445587N-(5-bromothiophenesulfonyl)pyrrole

생성물 1

HCID 22998523HCID 22998523, 화합물수율 93%

실험 절차

N-[5-(3-methoxyphenyl)thiophene-2-sulfonyl]pyrrole was prepared in the same manner as described in Example 32C from 3-methoxyphenylboronic acid and N-(5-bromothiophene-2-sulfonyl)pyrrole in 93% yield. This was purified by recrystallization using hexane/ethyl acetate as solvent.

후처리

  1. customThis was purified by recrystallization

출처 및 근거

ORD 기록
ord-f4509aa58e704c21a3b7b244031cc66e
출처 데이터셋
uspto-grants-1997_01
특허 번호
US05594021

연결된 노트

불러오는 중…