Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sulfuryl chloride → 2-[(4-Methylphenoxy)methyl]thiophene-3-sulfonyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sulfuryl chloride | HCID 24648 | — |
| 반응물 | Sodium hydroxide ethanol | HCID 23692425 | — |
| 반응물 | 2-[(4-Methylphenoxymethyl]thiophene-3-sulfonyl}pyrrole | HCID 86583961 | — |
| 생성물 | 2-[(4-Methylphenoxy)methyl]thiophene-3-sulfonyl chloride | HCID 23445257 | — |
반응 단계
2-[(4-methylphenoxy)methyl]thiophene-3-sulfonyl chloride was prepared, as described in Example 64E, using N-{2-[(4-methylphenoxymethyl]thiophene-3-sulfonyl}pyrrole by basic hydrolysis (NaOH/EtOH) followed by conversion to the corresponding sulfonyl chloride, in yield.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05594021 |
| 출처 데이터셋 | uspto-grants-1997_01 |
| ORD ID | ord-9f5b939a1dc144308375610f33650166 |
| 출처 메모 | uspto-grants-1997_01 |