Potassium Carbonate → 1-Bromo-2-fluoro-4-pentadecyloxybenzene

HRID 234554

반응식

HRID 234554 반응식
[Br:1][C:2]1[CH:7]=[CH:6][C:5]([OH:8])=[CH:4][C:3]=1[F:9].Br[CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH3:25].C(=O)([O-])[O-].[K+].[K+]>CC(=O)CC>[Br:1][C:2]1[CH:7]=[CH:6][C:5]([O:8][CH2:25][CH2:24][CH2:23][CH2:22][CH2:21][CH2:20][CH2:19][CH2:18][CH2:17][CH2:16][CH2:15][CH2:14][CH2:13][CH2:12][CH3:11])=[CH:4][C:3]=1[F:9]

참가 물질

5

반응물 3

HCID 11430Potassium CarbonateHCID 123941-BromopentadecaneHCID 27791534-Bromo-3-fluorophenol

생성물 1

HCID 233547141-Bromo-2-fluoro-4-pentadecyloxybenzene

시약·촉매·용매 1

HCID 6569Methyl Ethyl Ketone용매

실험 절차

This was prepared using a similar method to that described for compound 3. Quantities: compound 1 (2.31 g, 12.1 mmol), 1-bromopentadecane (3.97 g, 13.6 mmol), potassium carbonate (2.97 g, 21.5 mmol) and butanone (80 ml).

후처리

  1. customThis was prepared

출처 및 근거

ORD 기록
ord-5de064edf657453e8d674536104a3cca
출처 데이터셋
uspto-grants-1997_01
특허 번호
US05595682

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