Potassium Carbonate → 1-Bromo-2-fluoro-4-pentadecyloxybenzene
반응식
[Br:1][C:2]1[CH:7]=[CH:6][C:5]([OH:8])=[CH:4][C:3]=1[F:9].Br[CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH3:25].C(=O)([O-])[O-].[K+].[K+]>CC(=O)CC>[Br:1][C:2]1[CH:7]=[CH:6][C:5]([O:8][CH2:25][CH2:24][CH2:23][CH2:22][CH2:21][CH2:20][CH2:19][CH2:18][CH2:17][CH2:16][CH2:15][CH2:14][CH2:13][CH2:12][CH3:11])=[CH:4][C:3]=1[F:9]참가 물질
5
실험 절차
This was prepared using a similar method to that described for compound 3. Quantities: compound 1 (2.31 g, 12.1 mmol), 1-bromopentadecane (3.97 g, 13.6 mmol), potassium carbonate (2.97 g, 21.5 mmol) and butanone (80 ml).
후처리
- customThis was prepared
출처 및 근거
- ORD 기록
- ord-5de064edf657453e8d674536104a3cca
- 출처 데이터셋
- uspto-grants-1997_01
- 특허 번호
- US05595682
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