Nitric Acid → 1-Bromo-4-tert-butyl-2-nitrobenzene

HRID 23457

반응식

HRID 23457 반응식
[Br:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]([CH3:11])([CH3:10])[CH3:9])=[CH:4][CH:3]=1.[N+:12]([O-])([OH:14])=[O:13].S(=O)(=O)(O)O>C(O)(=O)C>[Br:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]([CH3:11])([CH3:10])[CH3:9])=[CH:4][C:3]=1[N+:12]([O-:14])=[O:13]

참가 물질

5

반응물 3

HCID 944Nitric AcidHCID 1118Sulfuric AcidHCID 775951-Bromo-4-tert-butylbenzene

생성물 1

HCID 112539061-Bromo-4-tert-butyl-2-nitrobenzene

시약·촉매·용매 1

HCID 176Acetic Acid용매

실험 절차

The reaction was done as described in General Method 12 using 1-bromo-4-tert-butyl-benzene (15 g), acetic acid (10 mL), nitric acid (6.5 g), and sulfuric acid (13 g). MS(APCI): 291.

출처 및 근거

ORD 기록
ord-a1396691bc9742e491510a81f6674e53
출처 데이터셋
uspto-grants-2005_02
특허 번호
US06852711B2

연결된 노트

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