Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Phosphate → 2-Amino-7-isopropyl-4-methyl-benzothiazole-6-thiol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Phosphate | HCID 1061 | — |
| 반응물 | D-1,4-Dithiothreitol | HCID 446094 | — |
| 반응물 | 7-Isopropyl-4-methyl-6-thiocyanato-benzothiazol-2-yl-amine | HCID 15473839 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 2-Amino-7-isopropyl-4-methyl-benzothiazole-6-thiol | HCID 22572907 | — |
반응 단계
The title compound was prepared according to General Method 14 using 7-isopropyl-4-methyl-6-thiocyanato-benzothiazol-2-yl-amine (Example L-5; 11.5 g, 43.7 mmol), dithiothreitol (27.0 g, 175 mmol), EtOH (200 mL), and phosphate buffer (50 mL). MS (APCI): 239 (M+H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06852711B2 |
| 출처 데이터셋 | uspto-grants-2005_02 |
| ORD ID | ord-10295e2b277a470283758c831ee5ebe7 |
| 출처 메모 | uspto-grants-2005_02 |