Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Phosphate → 2-Amino-6-tert-butyl-benzothiazole-4-thiol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Phosphate | HCID 1061 | — |
| 반응물 | D-1,4-Dithiothreitol | HCID 446094 | — |
| 반응물 | 6-Tert-butyl-4-thiocyanato-benzothiazol-2-yl-amine | HCID 15473842 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 2-Amino-6-tert-butyl-benzothiazole-4-thiol | HCID 22572780 | — |
반응 단계
The title compound was prepared according to General Method 14 using 6-tert-butyl-4-thiocyanato-benzothiazol-2-yl-amine (Example L-6; 2.0 g. 7.6 mmol), dithiothreitol (4.6 g, 30 mmol), phosphate buffer of pH 7 (10 mL), and EtOH (50 mL). The crude product was used further without any purification. MS (APCI): 239 (M+H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06852711B2 |
| 출처 데이터셋 | uspto-grants-2005_02 |
| ORD ID | ord-c023bb652b76466495c6fd9c9529320f |
| 출처 메모 | uspto-grants-2005_02 |