Phosphate → 2-(Methyloxycarbonyl)amino-4-isopropyl-7-methyl-benzothiazole-6-thiol

HRID 23463

반응식

HRID 23463 반응식
[CH3:1][O:2][C:3]([NH:5][C:6]1[S:7][C:8]2[C:14]([CH3:15])=[C:13]([S:16]C#N)[CH:12]=[C:11]([CH:19]([CH3:21])[CH3:20])[C:9]=2[N:10]=1)=[O:4].SC[C@H]([C@@H](CS)O)O.P([O-])([O-])([O-])=O>CCO>[CH3:1][O:2][C:3]([NH:5][C:6]1[S:7][C:8]2[C:14]([CH3:15])=[C:13]([SH:16])[CH:12]=[C:11]([CH:19]([CH3:21])[CH3:20])[C:9]=2[N:10]=1)=[O:4]

참가 물질

5

반응물 3

HCID 1061PhosphateHCID 446094D-1,4-DithiothreitolHCID 225730782-(Methyloxycarbonyl)amino-4-isopropyl-7-methyl-6-thiocyanato-benzothiazole

생성물 1

HCID 225729772-(Methyloxycarbonyl)amino-4-isopropyl-7-methyl-benzothiazole-6-thiol

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

The title compound was prepared according to General Method 14 using 2-(methyloxycarbonyl)amino-4-isopropyl-7-methyl-6-thiocyanato-benzothiazole (1.5 g, 4.7 mmol), dithiothreitol (2.9 g, 18.7 mmol), EtOH (50 mL), and phosphate buffer (15 mL). MS (APCI): 296 (M−H).

출처 및 근거

ORD 기록
ord-5b61d909b51a46b58d8de41f946ae5e3
출처 데이터셋
uspto-grants-2005_02
특허 번호
US06852711B2

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