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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 234804생성일: 2026년 10월 25일

Cinchomeronic acid → 1H,3H-furo(3,4-c)pyridine-1,3-dione

https://huagongshe.com/reaction/234804

반응식

참여 물질

역할이름HCID투입량
반응물Cinchomeronic acidHCID 10273—
용매Acetic AnhydrideHCID 7918—
생성물1H,3H-furo(3,4-c)pyridine-1,3-dioneHCID 27839875.5%

반응 단계

A mixture of pyridine 3,4-dicarboxylic acid (15.0 g) and acetic anhydride (30 mL) is refluxed for two hours. The excess acetic anhydride is removed by distillation and the anhydride is collected and purified by sublimation (123° C. at 3 mm Hg) to yield pyridine 3,4-dicarboxylic acid anhydride as a white solid (10.1 g).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05596097
출처 데이터셋uspto-grants-1997_01
ORD IDord-4dc1f62024d04909a387aae886214db3
출처 메모uspto-grants-1997_01