Ethyl sulfide → HCID 86743413, 화합물

반응식

[CH2:1]([S:3][CH2:4][CH3:5])[CH3:2].[CH2:6]([I:28])[CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH3:27]>>[I-:28].[CH2:1]([S+:3]([CH2:4][CH3:5])[CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH3:27])[CH3:2]

참가 물질

반응물 2

HCID 9609Ethyl sulfide

HCID 132572191-Iododocosane

생성물 1

HCID 86743413HCID 86743413, 화합물

실험 절차

Diethyl sulphide is quaternized by docosyl iodide in order to obtain diethyldocosylsulphonium iodide. This iodide is then placed in an alcoholic solution with an equivalent of the TCNQ lithium salt. This gives crystals, which are recrystallized in alcohol. These crystals are constituted by the simple tetracyanoquinodimethane diethyl docosyl sulphonium salt of formula: ##STR4##

출처 및 근거

ORD 기록: ord-c8b229f5aef446ccb6a3461411dca00c
출처 데이터셋: uspto-grants-1989_10
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04871680

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