HCID 13592035, 화합물 → 3-(5-Hydroxy-4,6,7-trimethyl-1,3-benzoxathiazol-2-yl)propanol

반응식

C(OC(CCC([O:10][C:11]1[C:12]([CH3:29])=[C:13]([CH3:28])[C:14]2[O:18][CH:17]([CH2:19][CH2:20][C:21](OCC)=[O:22])[S:16][C:15]=2[C:26]=1[CH3:27])=O)=O)C.C(OC1C(C)=C(C)C2OC(C)SC=2C=1C)(=O)C>>[OH:10][C:11]1[C:12]([CH3:29])=[C:13]([CH3:28])[C:14]2[O:18][CH:17]([CH2:19][CH2:20][CH2:21][OH:22])[S:16][C:15]=2[C:26]=1[CH3:27]

참가 물질

반응물 2

HCID 13592035HCID 13592035, 화합물

HCID 14802163HCID 14802163, 화합물

생성물 1

HCID 1275773-(5-Hydroxy-4,6,7-trimethyl-1,3-benzoxathiazol-2-yl)propanol

실험 절차

Ethyl 3-[5-(3-ethoxycarbonylpropionyloxy)-4,6,7-trimethyl-1,3-benzoxathiole-2-yl)propionate (prepared as described in Example 32) was used in the same process as described in (1) above, to give the title compound, whose melting point, infrared absorption spectrum and mass spectrum were the same as those of the product described in (a) above.

출처 및 근거

ORD 기록: ord-cc5b225bed534097ab040a37af0f7b85
출처 데이터셋: uspto-grants-1989_10
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04871762

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