Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sulfuric Acid → 2,4,5-Trifluorobenzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sulfuric Acid | HCID 1118 | — |
| 반응물 | 2,4,5-Trifluorobenzonitrile | HCID 593813 | — |
| 생성물 | 2,4,5-Trifluorobenzamide | HCID 2776958 | — |
반응 단계
In 20 ml of 80% sulfuric acid was dissolved 5.8 g of 2,4,5-trifluorobenzonitrile and the mixture was heated under reflux for 30 minutes. After cooling, the reaction mixture was poured into ice-water and extracted with ethyl acetate. The extract was dried over sodium sulfate and the solvent was removed to yield 5.32 g of 2,4,5-trifluorobenzamide.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04871852 |
| 출처 데이터셋 | uspto-grants-1989_10 |
| ORD ID | ord-02bb96cf642d4a6db1a242a2bebdc1e3 |
| 출처 메모 | uspto-grants-1989_10 |