Dicyclohexylcarbodiimide → 2-Dimethylaminopyridine

HRID 235208

반응식

HRID 235208 반응식
[CH3:1][C@H]1OC(=O)C2C(O)=CC(O)=C(Cl)C=2CC(=O)C=CC=C[C@H]2O[C@H]2C1.CC(CCCCCCCCCCCCC(O)=O)C.[CH:44]1([N:50]=[C:51]=[N:52][CH:53]2[CH2:58][CH2:57][CH2:56]CC2)CCCCC1>O1CCCC1>[CH3:1][N:50]([C:51]1[CH:56]=[CH:57][CH:58]=[CH:53][N:52]=1)[CH3:44]

참가 물질

5

반응물 3

HCID 10868DicyclohexylcarbodiimideHCID 3624714-Methylpentadecanoic acidHCID 11268547CID 11268547

생성물 1

HCID 218852-Dimethylaminopyridine

시약·촉매·용매 1

HCID 8028Tetrahydrofuran용매

실험 절차

Following a procedure similar to that described in Example 12, but using 500 mg of radicicol, 878 mg of isopalmitic acid, 20 ml of dry tetrahydrofuran, 848 mg of dicyclohexylcarbodiimide and a catalytic amount of dimethylaminopyridine, 1.12 g of the title compound were obtained.

출처 및 근거

ORD 기록
ord-1148c1edd43d4f6e91b5c4fc7957e60f
출처 데이터셋
uspto-grants-1997_01
특허 번호
US05597846

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