Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dicyclohexylcarbodiimide → 2-Dimethylaminopyridine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dicyclohexylcarbodiimide | HCID 10868 | — |
| 반응물 | CID 11268547 | HCID 11268547 | — |
| 반응물 | 12-{[(Prop-2-en-1-yloxy)carbonyl]amino}dodecanoic acid | HCID 11652337 | — |
| 용매 | N-methyl-2-pyrrolidone | HCID 13387 | — |
| 생성물 | 2-Dimethylaminopyridine | HCID 21885 | — |
반응 단계
Following a procedure similar to that described in Example 12, but using 547 mg of radicicol, 3.75 g of 12-allyloxycarbonylaminododecanoic acid, 15 ml of dry 1-methyl-2-pyrrolidinone, 1.6 g of dicyclohexylcarbodiimide and a catalytic amount of dimethylaminopyridine, 418 mg of the title compound were obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05597846 |
| 출처 데이터셋 | uspto-grants-1997_01 |
| ORD ID | ord-0d49396f87aa4d0694bd0c6068091e57 |
| 출처 메모 | uspto-grants-1997_01 |