HCID 14601402, 화합물 → HCID 14601407, 화합물

반응식

[CH3:1][O:2][CH2:3][CH2:4][NH:5][CH2:6][C:7]1[S:14][C:13]2[CH:12]=[C:11]([S:15]([NH2:18])(=[O:17])=[O:16])[S:10][C:9]=2[CH:8]=1.C(NCC1SC2C=C(S(N)(=O)=O)SC=2C=1)C(C)C.[ClH:37].C(NCC1SC2C=C(S(N)(=O)=O)SC=2C=1)C(C)C>>[ClH:37].[CH3:1][O:2][CH2:3][CH2:4][NH:5][CH2:6][C:7]1[S:14][C:13]2[CH:12]=[C:11]([S:15]([NH2:18])(=[O:17])=[O:16])[S:10][C:9]=2[CH:8]=1

참가 물질

반응물 3

HCID 14601402HCID 14601402, 화합물

HCID 146014065-{[(2-Methoxyethyl)amino]methyl}thieno[3,2-b]thiophene-2-sulfonamide

HCID 19844139HCID 19844139, 화합물

생성물 1

HCID 14601407HCID 14601407, 화합물

실험 절차

The procedure of Example I was followed except that in Step L 5-[(2-methoxy)ethylaminomethyl]thieno[3,2-b]thiophene-2-sulfonamide was substituted for 5-isobutylaminomethylthieno[3,2-b]thiophene-2-sulfonamide to give 0.46 g of 5-[(2-methoxy)ethylaminomethyl]thieno[3,2-b]thiophene-2-sulfonamide hydrochloride, mp 224°-225° C. (D).

출처 및 근거

ORD 기록: ord-b1ac14ff15004a28ab0013e0bfd646a2
출처 데이터셋: uspto-grants-1989_10
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04876271

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