Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
O-Phenylenediamine → HCID 178419295, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | O-Phenylenediamine | HCID 7243 | — |
| 반응물 | 1H-Indole-2,3-dione, 6-bromo- | HCID 95716 | — |
| 용매 | Butyric Acid | HCID 264 | — |
| 생성물 | HCID 178419295 | HCID 178419295 | — |
반응 단계
A solution of 15.18 g (67.2 mmol) of 6-bromoisatin and 7.26 g (1.0 eq.) of 1,2-phenylenediamine in 250 ml of butyric acid was refluxed for 4 hours, followed by allowing to stand at room temperature for 16 hours. The precipitate was collected by filtration to give 8-bromoindolo[2,3-b]quinoxaline.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05597921 |
| 출처 데이터셋 | uspto-grants-1997_01 |
| ORD ID | ord-8cf9452ba60643d19233af36ff4282ad |
| 출처 메모 | uspto-grants-1997_01 |