Water → HCID 178419936, 화합물

HRID 235276

반응식

HRID 235276 반응식
[C:1]([C:3]1[CH:12]=[CH:11][C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=1)#[N:2].[N-:13]=[N+:14]=[N-:15].[Na+].[Cl-].[Li+].O>COCCO>[CH:4]1[C:5]2[C:10](=[CH:9][CH:8]=[CH:7][CH:6]=2)[CH:11]=[CH:12][C:3]=1[C:1]1[NH:15][N:14]=[N:13][N:2]=1

참가 물질

6

반응물 4

HCID 962WaterHCID 119442-NaphthalenecarbonitrileHCID 33557Sodium AzideHCID 433294Lithium Chloride

생성물 1

HCID 178419936HCID 178419936, 화합물

시약·촉매·용매 1

HCID 80192-Methoxyethanol용매

실험 절차

A mixture of 10 g of 2-cyanonaphthalene, 10.61 g of sodium azide, and 7.67 g of lithium chloride was placed in a reaction vessel, and 240 ml of 2-methoxyethanol serving as a solvent was added thereto. The above mixture was refluxed with stirring for 80 hours. The mixture was cooled to room temperature, and 500 ml of water was added to the mixture.

후처리

  1. customwas placed in a reaction vessel
  2. temperatureThe above mixture was refluxed

출처 및 근거

ORD 기록
ord-137d0e3b02b449b0bb19965f452b207a
출처 데이터셋
uspto-grants-1997_01
특허 번호
US05597925

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