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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 235319생성일: 2026년 10월 26일

Methanol → 4-(3-tert-Butyl-4-methoxybenzoyloxyethyl)benzenemethanol

https://huagongshe.com/reaction/235319

반응식

참여 물질

역할이름HCID투입량
반응물MethanolHCID 887—
반응물TetrahydrofuranHCID 8028—
반응물Sodium borohydrideHCID 4311764—
반응물4-(3-tert-Butyl-4-methoxybenzoyloxymethyl)benzaldehydeHCID 21474525—
용매WaterHCID 962—
생성물4-(3-tert-Butyl-4-methoxybenzoyloxyethyl)benzenemethanolHCID 53848055—

반응 단계

1.6 g (5 mmol) of the aldehyde obtained in Example 45, 50 ml of THF and 50 ml of methanol are introduced into a round-bottomed flask. 100 mg (2.5 mmol) of sodium borohydride are added in small portions and the mixture is stirred at room temperature for 4 h. The reaction medium is poured into water, the mixture is extracted with ethyl ether and the organic phase is separated after settling has taken place, dried over magnesium sulphate and evaporated.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05597839
출처 데이터셋uspto-grants-1997_01
ORD IDord-9f4bd2205b2e42ceba968bdc02156d6e
출처 메모uspto-grants-1997_01