C(OC(N1C2C(=CC3OC(F)(F)OC=3C=2)[C@H](O)CCC1)=O)(C)(C)C.C1C=CC(P(N=[N+]=[N-])(C2C=CC=CC=2)=O)=CC=1.C1CCN2C(=NCCC2)CC1.[C:53]([O:57][C:58]([N:60]1[C:73]2[C:65](=[CH:66][C:67]3[O:68][C:69]([F:75])([F:74])[O:70][C:71]=3[CH:72]=2)[C@@H:64]([N:76]=[N+]=[N-])[CH2:63][CH2:62][CH2:61]1)=[O:59])([CH3:56])([CH3:55])[CH3:54]>C1(C)C=CC=CC=1.CO.[Pd]>[C:53]([O:57][C:58]([N:60]1[C:73]2[C:65](=[CH:66][C:67]3[O:68][C:69]([F:75])([F:74])[O:70][C:71]=3[CH:72]=2)[C@@H:64]([NH2:76])[CH2:63][CH2:62][CH2:61]1)=[O:59])([CH3:56])([CH3:54])[CH3:55]To a solution of (R)-2,2-Difluoro-9-hydroxy-6,7,8,9-tetrahydro-1,3-dioxa-5-aza-cyclohepta[f]indene-5-carboxylic acid tert-butyl ester (1.9 mmol) in Toluene, add DPPA (2.5 mmol) and DBU (2.5 mmol). After heating the mixture at 65° C. for 14 h, remove solvent under vacuum and chromatograph the intermediate using ethyl acetate/hexane (5-20%) to elute. This provides (S)-9-Azido-2,2-difluoro-6,7,8,9-tetrahydro-1,3-dioxa-5-aza-cyclohepta[f]indene-5-carboxylic acid tert-butyl ester as a colorless oil. To a solution of (S)-9-Azido-2,2-difluoro-6,7,8,9-tetrahydro-1,3-dioxa-5-aza-cyclohepta[f]indene-5-carboxylic acid tert-butyl ester (1.8 mmol) in methanol (20 mL) add a catalytic amount of Pd/C after purging the solution with nitrogen. Place a balloon of hydrogen on the reaction and purge the solution several times. After stirring for 1 h, purge the solution with nitrogen then filter through celite. Collect the filtrate and remove solvent under vacuum to provide the title compound as a colorless oil.
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