2-Ethenylbenzenesulfonamide → N-[(4,6-Dichloro-1,3,5-triazin-2-yl)aminocarbonyl]-2-ethenylbenzenesulfonamide

HRID 235568

반응식

HRID 235568 반응식
[Cl:1][C:2]1[N:7]=[C:6]([Cl:8])[N:5]=[C:4]([N:9]=[C:10]=[O:11])[N:3]=1.[CH:12]([C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][C:15]=1[S:20]([NH2:23])(=[O:22])=[O:21])=[CH2:13]>C(#N)C>[Cl:8][C:6]1[N:7]=[C:2]([Cl:1])[N:3]=[C:4]([NH:9][C:10]([NH:23][S:20]([C:15]2[CH:16]=[CH:17][CH:18]=[CH:19][C:14]=2[CH:12]=[CH2:13])(=[O:21])=[O:22])=[O:11])[N:5]=1

참가 물질

4

반응물 2

HCID 113674032-EthenylbenzenesulfonamideHCID 130526242,4-Dichloro-6-isocyanato-1,3,5-triazine

생성물 1

HCID 20218271N-[(4,6-Dichloro-1,3,5-triazin-2-yl)aminocarbonyl]-2-ethenylbenzenesulfonamide

시약·촉매·용매 1

HCID 6342Acetonitrile용매

실험 절차

A solution of 4,6-dichloro-1,3,5-triazin-2-yl isocyanate (0.87 g, 4.5 mmol) in acetonitrile (9 ml) is contacted with 2-ethenylbenzenesulfonamide (0.83 g, 4.5 mmol) and stirred for 16 hours. The mixture is then evaporated under reduced pressure to yield the title compound which is used directly in subsequent reactions.

후처리

  1. customThe mixture is then evaporated under reduced pressure

출처 및 근거

ORD 기록
ord-1df3afabf3e9489b97b7a1acc5d394dd
출처 데이터셋
uspto-grants-1987_02
특허 번호
US04640704

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