Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrogen Bromide → 2,6-Diphenylpyridine hydrobromide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrogen Bromide | HCID 260 | — |
| 반응물 | 2,6-Diphenylpyridine | HCID 72920 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | 2,6-Diphenylpyridine hydrobromide | HCID 20218321 | — |
반응 단계
Hydrogen bromide gas is introduced into a solution of 30 g (0.130 mole) of 2,6-diphenylpyridine in 150 ml of toluene. The solid which forms is isolated by vacuum filtration. The filtrate is retreated with hydrogen bromide until no more solid is formed. The solid is then dried in vacuo. The product has a melting point of 161° C.-162° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04640831 |
| 출처 데이터셋 | uspto-grants-1987_02 |
| ORD ID | ord-60faa63473cd46718136fe30ba636c9d |
| 출처 메모 | uspto-grants-1987_02 |