Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Pyridineethanamine → HCID 16036094, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Pyridineethanamine | HCID 75919 | — |
| 반응물 | 6-{4-[2-(Trifluoromethyl)benzoyl]piperazin-1-yl}pyridazine-3-carbonyl chloride | HCID 86597230 | — |
| 생성물 | HCID 16036094 | HCID 16036094 | — |
반응 단계
Following the procedure of Example 28, making variations only as required to use 2-pyridin-2-ylethylamine in place of 2-aminopyridine to react with 6-[4-(2-trifluoromethyl-benzoyl)piperazin-1-yl]pyridazine-3-carbonyl chloride, the title compound was obtained as a white powder (30%). m.p. 151-154° C. 1H NMR (300 MHz, DMSO-d6) δ 9.07, 8.78, 8.43, 7.99-7.61, 7.52, 7.34, 3.79-3.60, 3.35-3.14. MS (ES+) m/z 485.3 (M+1).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07759348B2 |
| 출처 데이터셋 | uspto-grants-2010_07 |
| ORD ID | ord-88fa727b1f9344319d056aa930f93651 |
| 출처 메모 | uspto-grants-2010_07 |