참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Pyridine | HCID 1049 | — |
| 반응물 | Methacrylic anhydride | HCID 12974 | — |
| 반응물 | 2-Dimethylaminopyridine | HCID 21885 | — |
| 반응물 | Allyloxypropanediol | HCID 22483925 | — |
| 용매 | Chloroform | HCID 6212 | — |
| 생성물 | Allyloxypropanediol Dimethacrylate | HCID 20220160 | — |
반응 단계
Allyloxypropanediol (0.5 equivalents) was stirred in chloroform with pyridine (1 equivalent) and dimethlaminopyridine (0.05 equivalent) and warmed to 50° C. Methacrylic anhydride was added dropwise and stirring was continued until starting diol was no longer detected by gas chromatography. The reaction mixture was then washed with dilute hydrochloric acid, sodium bicarbonate and water. Concentration on a rotary evaporator gave the crude product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04640940 |
|---|
| 출처 데이터셋 | uspto-grants-1987_02 |
|---|
| ORD ID | ord-bdfe362f90b5432f81952ef2a1d2d655 |
|---|
| 출처 메모 | uspto-grants-1987_02 |
|---|
