Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → 2-(3-Methoxyphenyl)cyclopropane-1-carboxylic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Cyclopropanecarboxylic acid, 2-(3-methoxyphenyl)-, ethyl ester | HCID 19358490 | — |
| 용매 | Ethanol | HCID 702 | — |
| 용매 | Sodium Hydroxide | HCID 14798 | — |
| 생성물 | 2-(3-Methoxyphenyl)cyclopropane-1-carboxylic acid | HCID 13972233 | — |
반응 단계
The crude 2-(3-methoxy-phenyl)-cyclopropanecarboxylic acid ethyl ester is dissolved in 30 ml EtOH and 15 ml 1N NaOH. After stirring over night, the reaction mixture is acidified with 1N HCl and extracted with diethyl ether. After removal of the solvent 7.1 g of the 2-(3-methoxy-phenyl)-cyclopropanecarboxylic acid is obtained. This 2-(3-methoxy-phenyl)-cyclopropanecarboxylic acid is used without further purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07763728B2 |
| 출처 데이터셋 | uspto-grants-2010_07 |
| ORD ID | ord-115159adedc34e79819ccca64391392a |
| 출처 메모 | uspto-grants-2010_07 |