참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Ethyl chloroacetate | HCID 7751 | — |
| 반응물 | Carbonic acid, methyl phenyl ester | HCID 139482 | — |
| 반응물 | Tbpb | HCID 10092649 | — |
| 생성물 | Acetic acid, 2-phenoxy-, ethyl ester | HCID 17365 | 96% |
반응 단계
A mixture of 3.8 g of methyl phenyl carbonate, 3.06 g of ethyl chloroacetate, and 0.42 g of TBPB was heated at 120° C. for 2 hours. Distillation of the resulting reaction mixture provided a 96 percent yield of ethyl phenoxyacetate.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04642349 |
|---|
| 출처 데이터셋 | uspto-grants-1987_02 |
|---|
| ORD ID | ord-84617750b2de451891c31139817feac1 |
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| 출처 메모 | uspto-grants-1987_02 |
|---|
