Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Pyridine → Methyl 3,5,6-trichloro-2-pyridyl carbonate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Pyridine | HCID 1049 | — |
| 반응물 | Methyl chloroformate | HCID 6586 | — |
| 반응물 | HCID 178517807 | HCID 178517807 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | Methyl 3,5,6-trichloro-2-pyridyl carbonate | HCID 20218094 | — |
반응 단계
Methyl 3,5,6-trichloro-2-pyridyl carbonate was prepared by reacting methyl chloroformate with 3,5,6-trichloro-2-pyridinol at 0° C.-5° C. in the presence of an equivalent of pyridine as acid acceptor and using methylene chloride as the reaction solvent.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04642349 |
| 출처 데이터셋 | uspto-grants-1987_02 |
| ORD ID | ord-dfd40673d47e474b829ec112e5888f72 |
| 출처 메모 | uspto-grants-1987_02 |