Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Hydroxide → (2-Bromophenyl)hydrazine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | 2-Bromophenylhydrazine hydrochloride | HCID 2723912 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | (2-Bromophenyl)hydrazine | HCID 85583 | — |
반응 단계
15 g 2-bromophenylhydrazine hydrochloride are suspended in 400 ml of toluene and combined with 240 ml of 1 N sodium hydroxide solution. The mixture is stirred for 1 hour and the phases are separated. The organic phase is dried on magnesium sulphate and the solvents are eliminated in vacuo. The crude product thus obtained is further reacted directly.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08686022B2 |
| 출처 데이터셋 | uspto-grants-2014_04 |
| ORD ID | ord-15172afbc4084c749fa1d4454ea24d19 |
| 출처 메모 | uspto-grants-2014_04 |