4-Phenylthiocyclohexanone Oxime → HCID 20217891, 화합물
반응식
[C:1]1([S:7][CH:8]2[CH2:13][CH2:12][C:11](=[N:14]O)[CH2:10][CH2:9]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[H-].C([Al+]CC(C)C)C(C)C>C(Cl)Cl>[C:1]1([S:7][CH:8]2[CH2:13][CH2:12][CH2:11][NH:14][CH2:10][CH2:9]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1참가 물질
4
실험 절차
Following an analogous procedure to that of Sasatani, S. et al. described in Tetrahedron Letters, Vol. 24 (No. 43), pp 4711-4712 (1982), 4-phenylthiocyclohexanone oxime is reacted with diisobutyl aluminum hydride in methylene chloride to give the title compound.
출처 및 근거
- ORD 기록
- ord-003f739b4cc34785830a189acfed03aa
- 출처 데이터셋
- uspto-grants-1987_02
- 특허 번호
- US04642348
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