Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Diethanolamine → HCID 22590162, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Diethanolamine | HCID 8113 | — |
| 반응물 | 4-Fluoro-3-(trifluoromethyl)benzonitrile | HCID 144255 | — |
| 용매 | Dimethylacetamide | HCID 31374 | — |
| 생성물 | HCID 22590162 | HCID 22590162 | — |
반응 단계
A solution of 3-trifluoromethyl 4-fluoro-benzonitrile (9.45 g, 50 mmol) and diethanolamine (15.8 g, 0.15 mol) in N,N-dimethylacetamide (200 ml) was stirred for 7 days at 50° C. The solvent was evaporated, the residue partitioned between CH2Cl2 (400 ml) and H2O (400 ml), the organic layer dried (MgSO4) and evaporated to dryness. The residue was chromatographed using CH2Cl2-EtOH as eluent.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06852755B1 |
| 출처 데이터셋 | uspto-grants-2005_02 |
| ORD ID | ord-02ab42cfd43b416bbf1faed23df2983f |
| 출처 메모 | uspto-grants-2005_02 |