Ammonia → 3-Amino-1,2,4-triazine mesylate

HRID 2361859노트

반응식

HRID 2361859 반응식
C(OC1C=C(C=[CH:17][CH:18]=1)C(OC)=O)C1C=CC=CC=1.[S:19]([OH:23])(=[O:22])(=[O:21])[CH3:20].S(O)(=O)(=O)C.[NH2:29][NH:30][C:31]([NH2:33])=[NH:32].N>>[S:19]([OH:23])(=[O:22])(=[O:21])[CH3:20].[NH2:33][C:31]1[N:30]=[N:29][CH:17]=[CH:18][N:32]=1

참가 물질

4

반응물 3

HCID 222AmmoniaHCID 13368031Methyl 3-(benzyloxy)benzoateHCID 178505340HCID 178505340, 화합물

생성물 1

HCID 866497313-Amino-1,2,4-triazine mesylate

실험 절차

Prepared by reacting acenaphthenequinone (3) with aminoguanidine bismesylate for 24 hrs using the above procedure except that the basification step with ammonia was omitted. The title compound was obtained as bright yellow prisms in 83.2%, mpt=264-266° (froth)

후처리

  1. customPrepared
  2. customfor 24 hrs

출처 및 근거

ORD 기록
ord-be71e0b7da95491687df91d7870b06c0
출처 데이터셋
uspto-grants-2014_04
특허 번호
US08691818B2

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