Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Catechol → HCID 11820088, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Catechol | HCID 289 | — |
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | Ethyl dichlorophosphate | HCID 15158 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 생성물 | HCID 11820088 | HCID 11820088 | 95.1% |
반응 단계
Pyrocatechol (1.249 g, 11.35 mM) was dissolved in 42 ml of ether and, using 2.297 g (22.70 mM) of triethylamine and 1.849 g (11.35 mM) of ethyl dichlorophosphate, the reaction was carried out at -40° C. to -35° C. and the reaction mixture treated in the same manner as in Reference Example 1. There was obtained 2.159 g (95.0% yield) of ethyl o-phenylene phosphate as a colorless viscous oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04642365 |
| 출처 데이터셋 | uspto-grants-1987_02 |
| ORD ID | ord-5614493c1a0c4f8f99a799246d8cd8e7 |
| 출처 메모 | uspto-grants-1987_02 |